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Scope & Range of Services
Academic Experience:
1998 - present
Associate Professor, Materials Science & Engineering Department, Iowa
State University.
1992 - 1998
Assistant Professor, Materials Science & Engineering Department, Iowa
State Unversity.
1988 - 1992
Teaching Assistant, University of Washington. T. A. for sequence of two,
junior-level courses in Ceramic Engineering. Also served as grader for
graduate course in the mechanical behavior of composites.
1981 - 1983
Teaching Assistant, U.C.L.A. T.A. in introductory materials science class
and an undergraduate class in diffusion in solids.
Industrial Experience:
1992 - present
Associate, Metallurgy & Ceramics Division of the Ames Laboratory, Ames,
IA
1986 - 1992
Senior Research Engineer, Battelle-Northwest Laboratories, Richland, WA.
Research activities were in three areas: 1) development of a radiographic
method to analyze effects of suspension chemistry variables on ceramic
powder compaction, 2) development of processing methods to strengthen
SiC-fiber-reinforced silicon nitride, and 3) testing of TiB2-based cathodes
for degradation mechanisms during the electrolytic production of aluminum.
Primary responsibilities included proposal and report preparation, project
planning, and management of laboratory research. Dr. Schilling was
employed half time from 8/88 to 3/92 while earning his Ph.D.
1984 - 1986
Research Engineer, N.A.S.A. Jet Propulsion Laboratory, Pasadena, CA.
Responsibilities included 1) design and operation of a drop tube facility
for
solidification processing of glass, metal, and polymeric microballoons,
2)
development of experimental methods to evaluate microballoon flaws (e.g.,
SEM/EDS, x-ray radiography), and 3) mechanical design of an acoustic
levitation system to study containerless solidification.
1974 - 1976
Machinist, X.R.E. Corporation, Littleton, MA.
Performed lathe and milling operations while apprenticing in a shop making
prototype medical x-ray equipment. Dr. Schilling took pre-engineering
courses while enrolled in a co-op program at Northeastern University.
Research Description:
Surface chemical and rheological
aspects of ceramic shape-forming (slipcasting, gelcasting,
injection molding, filtration,
and tape casting).
The use of nondestructive evaluation
to analyze formation of green body defects (porosity
gradients, composition gradients)
during shape-forming of ceramics.
Fundamental aspects of the mechanics
of particulate media.
Processing of ceramic hard coatings.
Mechanical behavior of materials.
Teaching:
Undergraduate:
MSE 402L Mechanical Metallurgy
Lab, F92
MSE 307L Pyrometry and Thermal
Processing of Ceramics Lab, S93, S95, S96
MSE 405 Mechanical Behavior of
Materials, S94, S95, S96, S97, S98, S99
MSE 405L Mechanical Behavior of
Materials Lab, S94, S95, S96, S98, S99
MSE 420 Design for Thermal Processing,
F94, co-taught with D. Martin
MSE 406 Mechanical Metallurgy,
F98
MSE 406L Mechanical Metallurgy
Lab, F97, F98
Graduate:
MSE 576 Ceramic Processing, F93
MSE 603X Mathematical Methods in
Materials Research, F95
MSE 563 Powder Processing of Materials,
F96, F97
Future Thesis Topics:
X-ray nondestructive evaluation
of tape cast ceramics and ceramic composites.
X-ray absorption and fluid mechanics
analysis to measure the drained compressibility of colloidal
ceramic suspensions. This is a
rapid, quality control technique to screen the effects of ceramic
processing variables on their
tendency to form density gradients during slip casting, pressure
filtration, and centrifugal casting.
These gradients are a common source of cracks which degrade
the strength of ceramics.
High resolution x-ray tomography
to image 3-D density gradients in ceramic green bodies. We
use this technique to evaluate
microstructure evolution of green bodies during slurry
consolidation. Using economical,
"off the shelf" equipment, we can achieve high resolution, high
contrast imaging without the need
of costly, traditional methods (e.g., synchrotron radiation).
Studies focus in two areas: (1)
the development of new x-ray imaging methodologies, and (2)
developing a stronger, fundamental
understanding of the role of colloidal chemistry variables on
microstructure evolution during
consolidation.
Development of advanced methods
of shape-forming technical ceramics by gelcasting with
polysaccharides. Polysaccharides
are sugar molecules that eliminate the need for toxic organic
chemicals in traditional molding
operations such as tape casting and injection molding. Studies
focus on surface chemical aspects
of the crosslinking and flow behavior of colloidal ceramic
suspensions containing polysaccharides.
Honors/Awards:
Awarded Outstanding Young Engineering
Researcher by the College of Engineering at Iowa State
University, May 1998.
First place was awarded to N. T.
Saenz, C. H. Schilling, and J. W. Wald at the metallography
contest held by the International
Metallographic Society and the American Society for Metals,
July 23-27, 1989, Charlotte, N.C.
The title of the poster was "Analysis of SiC fiber reinforced
SiC matrix composites using transmission
optical microscopy."
Third place was awarded to N. T.
Saenz, W. J. Weber, and C. H. Schilling at the ceramography
contest held at the 1988 annual
meeting of the American Ceramic Society. The poster was
entitled, "Transmission Optical
Microscopy of SiC Fiber-Reinforced Si3N4."
Second place was awarded to N.
T. Saenz, R. H. Jones, C. H. Schilling and J. L. Bates at the
ceramography contest held by the
American Ceramic Society, April 1989, Indianapolis, IN. The
title of the poster was "Transmission
Optical Microscopy of SiC Reinforced SiC Composites."
This poster appeared on the cover
of the September 1989 issue of the Journal of the American
Ceramic Society.
Second place was awarded to N.
T. Saenz, C. H. Schilling, D. H. Parks, and G. L. Graff at the
metallography contest held by
the International Metallographic Society and the American Society
for Metals, July 23-27, 1989,
Charlotte, N.C. The title of the poster was "Aluminum Penetration
in TiB2 graphite Composites."
Gamma-ray densitometry, a nondestructive
analysis technique developed by Dr. Schilling at
Battelle was featured in a review
article on emerging methods for characterizing ceramics: L. M.
Sheppard, "Microanalysis: Solving
Microstructural Mysteries," Am. Cer. Soc. Bull., Vol. 68, No.
6, pp. 1187-1195, 1989.
Tau Beta Pi, National Engineering
Honor Society, Student Member.
Pi Tau Sigma, National Mechanical
Engineering Honor Society, President of Cal Poly Pomona
Student Chapter, 1981.
Sigma Xi, The Scientific Research
Society, Member.
Recent Publications:
Sikora, M., Schilling, C. H., Garcia,
V., Li, C. P., and Tomasik, P., "Effects of polysaccharide
concentration and molecular weight
on the rheology of alumina suspensions," submitted to J. Am.
Ceram. Soc. 9/98.
Tomasik, P., Schilling, C. H.,
Anderegg, J., and Refvik, M., "Lanthanum starchate," submitted
to Carbohydrate Polymers, 6/88.
Schilling, C. H., Garcia, V., Smith,
R. M., and Roberts, R. A., "Ultrasonic and mechanical
behavior of green- and partially-sintered
alumina: effects of slurry consolidation chemistry," J.
Am. Ceram. Soc. , Vol. 81, No.
10, pp. 2629-39 (1998).
Garcia, V. J. and Schilling, C.
H., "Ultrasonic velocity and reduction of surface area during solid
state sintering," accepted in
Materials Science and Engineering, A, 11/98.
Schilling, C. H., Bellman, R.,
Smith, R. M., Goel, H., and Giesche, H., "Plasticizing aqueous
suspensions of concentrated alumina
with maltodextrin sugar," accepted 8/98 in J. Am. Ceram.
Soc.
Tomasik, P. and Schilling, C. H.,
"Chemical modification of starch," submitted to Advances in
Carbohydrate Chemistry and Biochemistry,
11/98.
Tomasik, P. and Schilling, C. H.,
"Starch complexes, Part 1: complexes with inorganic guests,"
Advances in Carbohydrate Chemistry
and Biochemistry, Volume 53, pp. 263-343 (1998).
Tomasik, P. and Schilling, C. H.,
"Starch Complexes, Part 2: complexes with organic guests,"
Advances in Carbohydrate Chemistry
and Biochemistry, Volume 53, pp. 345-426 (1998).
Garcia, V. J., Schilling, C. H.,
Huss, S. P., Gray, J. N., Sikora, M., Tomasik, P., the Li, C. P.,
"X-ray NDE of density gradients
during alumina powder consolidation: effects of suspension
chemistry," in Proceedings of
the American Ceramic Society Symposium on Advances in
Process Measurements for the Ceramic
Industry, Cincinatti, OH, May 3 - 6, 1998, in press.
Schilling, C. H., Tomasik, P.,
Sikora, M., Kim, J. C., Garcia, V. J., and Li, C. P., "Molding
technical ceramics with polysaccharides,"
in Proceedings of the Eighth International Starch
Conference, Krakow, Poland, June
16 - 19, 1998, in press.
Schilling, C. H., Gray, J. N.,
and Huss, S. P., "Needs and opportunities for NDE in ceramic
processing," in Ceramic Transactions,
Volume 67: Nondestructive Evaluation of Ceramics, edited
by Schilling, C. H. and Gray,
J. N. (American Ceramic Society, Westerville, Ohio, 1998), pp.
1-19.
Schilling, C. H., Gray, J. N.,
Huss, S. P., and Maranville, C. W., "Recent advances in x-ray
characterization of composites
and tape cast ceramics," in Ceramic Transactions, Volume 67:
Nondestructive Evaluation of Ceramics,
edited by Schilling, C. H. and Gray, J. N. (American
Ceramic Society, Westerville,
Ohio, 1998), pp. 45-58.
Huss, S. P., Gray, J. N., and Schilling,
C. H., "Fine scale resolution of ceramic microstructures
by x-ray computed tomography:
an economical approach," in Ceramic Transactions, Volume 67:
Nondestructive Evaluation of Ceramics,
edited by Schilling, C. H. and Gray, J. N. (American
Ceramic Society, Westerville,
Ohio, 1998), pp. 59-66.
Garcia, V. and Schilling, C. H.,
"Models relating ultrasonic velocity to the microstructures of
green and sintered ceramics: a
review," in Ceramic Transactions, Volume 67: Nondestructive
Evaluation of Ceramics, C. H.
Schilling and J. N. Gray, editors, American Ceramic Society,
Westerville, Ohio, 1998, 67-84.
Garcia, V. J., Martinez, L., Briceno-Valero,
J. M., and Schilling, C. H., "Dimensional metrology
of nanometric spherical particles
using AFM," Probe Mircoscopy, Vol. 1, pp. 107-116 (1997).
Garcia, V. J., Martinez, L., Briceno-Valero,
J. M., and Schilling, C. H., "Dimensional metrology
of nanometric spherical particles
using AFM, II, application of model - tapping mode" Probe
Mircoscopy, Vol. 10, pp. 117-125
(1998).
Patents:
An invention disclosure was filed
with the Center for Advanced Technology Development at
Iowa State University concerning
the use of a nondestructive technique to measure density
gradients in ceramics, 1998. Two
invention disclosures were also filed with the Center for
Advanced Technology Development
at Iowa State University concerning the use of starch
additives for aqueous colloidal
processing of particulate metals and ceramics, 1993.
Table of Contents:
Needs and Opportunities for NDE in Ceramic Processing. pp.
1-22. by C. H. Schilling and J.N. Gray.
Ultrasonic Wave Interactions with Colloidal Mixtures. pp.
23-32. by R. Challis and J. Tebbutt.
Ultrasonic Array Sensing for In-Situ NDE in Extrusion
Process. pp. 33-44. by T. Watanabe, T. Aizawe. and J. Kihara.
Recent Advances in X-ray Characterization of Composites and
Tape Cast Ceramics. pp.45-58. by S.P. Huss, C. H. Schilling, J.N.
Gray and C.W. Maranville.
Fine-Scale Resolution of Microscopic Feature by X-ray
Computed Tomography: An Economical Approach. pp.59-66.
by S.P. Huss, J.N. Gray and C. H. Schilling.
Models Relating Ultrasonic Velocity to the Microstructures of
Green and Sintered Ceramics: A Review
pp.67-84. by V.J. Garcia and C. H. Schilling.
In situ Measurement of Ultrasonic Sound Wave Velocity
During Sintering of Ceramic Powders. pp. 85-96. by L.P.
Martin, D. Dandon, and M. Rosen.
Relationship Between Specific Surface Area and Ultrasonic
Sound Wave Velocity in Sintered Ceramic Powders. pp. 97-108.
by L.P. Martin, D. Nagle, and M. Rosen.
Ultrasonic NDE of Fine Ceramics with Reference Test Pieces.
pp. 109-120. by Yasushi Ikeda, Yastoshi Mizuta, Katsuhiro Onda,
Hitoshi Domon, and Takashi Udagawa.
Nondestructive Evaluation of Woven Fabric Reinforced
Ceramic Composites. pp.121-136. by P.K. Liaw, J. Kim, N.
Miriyala, D.K. Hsu, N. Yu, D.J. McGuire, and W.A Simpson, Jr.
Ultrasonic Characterization of Microware-Joined Silicon
Carbide/Silicon Carbide. pp. 137-144. by Michael B. House and
Paul S. Day.
Nondestructive Evaluation of Brittle-Matrix Composites
During Loading by Electrical Resistance Measurment.
pp.145-158. by Shoukai Wang, Xuli Fu, and D.D.L. Chung.
Quantitative Nondestructive Evaluation of Surface Roughness
Using Ultrasonic Reflectivity and Surface Wave Velocity.
pp.159-170. by Tatsuhiko Aizawa and Ikuo Ihara.
Microscopic Characterization of Machined High-Performance
Ceramics Using Acoustical, Optical, and Mechanical NDT.
pp.171-182. by V. Scherer, S.U. Fassbender, G. Weides, and W.
Arnold.
Acoustic Spectro-Microscopy for Quantitative Nondestructive
Evaluation of Ceramic Coated Materials. pp.183-194. by
Tatsuhiko Aizawa.
Surface and Subsurface Flaw Detection in Silicon Nitride Using
Acoustic Microscopy. pp.195-204. by Pramod Khandelwal.
Grain Boundary Characterization and Evaluation by Acoustic
Spectro Microscopy. pp.205-216. by Y. Xu and Tatsuhiko
Aizawa.
Process Control of CVD Fiber Coatings. pp.217-228. by J.G.
Jones, P.D. Jero, and D.J. Kent.
Piezospectroscopic Characterization of Thermal Barrier
Coatings. pp.229-240. by M.J. Lance, J. Allen Haynes, W. Roger
Cannon, and Mattison K. Ferber
Ultrasonic Velocity Measurement of Molten Liquids.
pp.241-252. by R. Daniel Costley, W.M. Ingham, and Jason A.
Simpson.
Thickness-Independent Ultrasonic Imaging Applied to Ceramic
Materials. pp.253-264. by Don J. Roth and Dorothy V. Carney.
Non-Contact Ultrasonic Characterization of Ceramics and
Composites. pp.265-282. by Mahesh C. Bhardwaj.
X-ray NDE of Fine Ceramics With Image Subtraction Method.
pp.283-290. by Yasushi Ikeda, Yastoshi Mizuta, and Katsuhiro
Onda.
Sonic Detection of Manufacturing Flaws in Cermic
Components. pp.291-302. by David A. Pape.
Acoustic Emission Study of Microcracking in Whiteware.
pp.303-314. by Darren Stohe, Vernon Burdick, and James Varner.
Effect of the Degree of Domain Reversal on Acoustic Emission
in 1 mol% MnO2-Doped (Pb.85 La.15)TiO3 Ferroelectric
Ceramics. pp.315-326. by D.G. Choi and L.D. Pye.
Light Scattering of Particles in Glasses. pp.327-336. by M.H.
Goller and L.D. Pye
Elastic Modulus Calculations From Load/Displacement Curves
Using Spherical and Pointed Indentars. pp.337-344. by L.
Riester, M.K. Ferber, and K. Breder
Summary of Chris Schilling's
Articles
Energy dispersive radiography
for the simultaneous mapping of
porosity, composition, and
thickness of tape-cast ceramics and ceramic
composites.
X-ray absorption and fluid
mechanics analysis to measure the drained
compressibility of colloidal
ceramic suspensions. This is a rapid, quality
control technique to screen
the effects of suspension processing
variables on their tendency
to form density gradients during slip
casting, pressure filtration,
and centrifugal casting.
High resolution x-ray tomography
to image 3-D density gradients in
ceramic green bodies. We
use this technique to evaluate microstructure
evolution of green bodies
during slurry consolidation. Using
economical, "off the shelf"
equipment, we can achieve high resolution,
high contrast imaging without
the need of costly, traditional methods
(e.g., synchrotron radiation).
Works Cited:
Editor: Schilling, Christopher H. and Joseph N. Gray.
Nondestructive Evaluation of Ceramics(Ceramics Transactions
V. 89) Westerville, Ohio: The American Ceramic Society. ISBN:
1-57498-037-8. 1998. |